HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(+-)-1-Aminoindan → HCID 18627820, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (+-)-1-Aminoindan | HCID 123445 | — |
| Edukt | 4-(Dipropylsulfamoyl)benzoyl chloride | HCID 2735528 | — |
| Produkt | HCID 18627820 | HCID 18627820 | 63% |
Reaktionsschritte
The title compound was prepared in 63% yield from (rac)-1-aminoindan (10.0 g, 75.2 mmole) and 4-(di-n-propylsulfamoyl) benzoyl chloride (16.3 g, 53.6 mmole, prepared from probenecid and SOCl2) via a procedure analogous to that described in Ex. 46, followed by crystallization from hexane:EtOAc, mp: 124°-5° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05880159 |
| Quelldatensatz | uspto-grants-1999_03 |
| ORD ID | ord-37205c879f7d488baa7134d7dd3f956d |
| Quellennotiz | uspto-grants-1999_03 |