HCID 19348652, compound → HCID 19348558, compound

HRID 1418147Notes

Reaction equation

HRID 1418147 reaction equation
[C:1]([C:5]1[CH:10]=[CH:9][C:8]([C:11](=[O:13])[NH2:12])=[CH:7][C:6]=1[NH:14][C:15](=[O:39])[CH2:16][CH:17]([C:23]1[CH:28]=[CH:27][CH:26]=[C:25]([O:29][CH3:30])[C:24]=1[O:31]CC1C=CC=CC=1)[CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])([CH3:4])([CH3:3])[CH3:2]>C(OCC)C>[C:1]([C:5]1[CH:10]=[CH:9][C:8]([C:11](=[O:13])[NH2:12])=[CH:7][C:6]=1[NH:14][C:15](=[O:39])[CH2:16][CH:17]([C:23]1[CH:28]=[CH:27][CH:26]=[C:25]([O:29][CH3:30])[C:24]=1[OH:31])[CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])([CH3:2])([CH3:3])[CH3:4]

Participants

3

Reactant 1

HCID 19348652HCID 19348652, compound

Product 1

HCID 19348558HCID 19348558, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Following a similar procedure to that described in Preparation 124, but using N-(2-t-butyl-5-carbamoylphenyl)-3-(2-benzyloxy-3-methoxyphenyl)-octanamide (prepared as described in Example 119), the title compound was obtained as crystals, melting at 118°-121° C. (from diethyl ether).

Workup

  1. customthat described in Preparation 124

Sources & evidence

ORD record
ord-2d621511f33d4272a823e415ecd527d3
Source dataset
uspto-grants-1999_03
Patent number
US05880147

Reaction notes

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