HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-t-Butyl-5-cyano-1-nitrobenzene → Benzonitrile, 3-amino-4-(1,1-dimethylethyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-t-Butyl-5-cyano-1-nitrobenzene | HCID 10703362 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | Benzonitrile, 3-amino-4-(1,1-dimethylethyl)- | HCID 10702388 | — |
Reaction Steps
2-t-Butyl-5-cyano-1-nitrobenzene [prepared as described in step (i) above] was reduced in a similar manner to that described in Preparation 5 to give the title compound as crystals, melting at 94.5°-95° C. (from hexane-ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05880147 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-16a9739e907843e6b1d4f64b25e10041 |
| Source note | uspto-grants-1999_03 |