HCID 35370604, compound → HCID 67568297, compound

HRID 1418383Notes

Reaction equation

HRID 1418383 reaction equation
[ClH:1].Cl.[NH2:3][C:4]1[CH:12]=[CH:11][CH:10]=[C:9]([O:13][CH3:14])[C:5]=1[C:6]([NH2:8])=[NH:7].C1O[C:18]2([CH2:23][CH2:22][N:21]([C:24](=[O:33])[C:25]3[CH:30]=[CH:29][C:28]([C:31]#[N:32])=[CH:27][CH:26]=3)[CH2:20][CH2:19]2)OC1>>[ClH:1].[C:31]([C:28]1[CH:27]=[CH:26][C:25]([C:24]([N:21]2[CH2:22][CH2:23][C:18]3([N:7]=[C:6]([NH2:8])[C:5]4[C:4](=[CH:12][CH:11]=[CH:10][C:9]=4[O:13][CH3:14])[NH:3]3)[CH2:19][CH2:20]2)=[O:33])=[CH:30][CH:29]=1)#[N:32]

Participants

3

Reactant 2

HCID 35370604HCID 35370604, compoundHCID 67568446HCID 67568446, compound

Product 1

HCID 67568297HCID 67568297, compound

Procedure

This was prepared with 2-amino-6-methoxybenzamidine dihydrochloride (Example E) and 1-(4-cyanobenzoyl)-4-piperidone ethylene ketal by the method of Example 1 to give the title compound as a yellow solid, m.p. 252°-253° C.

Sources & evidence

ORD record
ord-da3d2faebbf3476bac17424ba5cf47a2
Source dataset
uspto-grants-1999_03
Patent number
US05883102

Reaction notes

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