HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl Isothiocyanate → 4-Allyl-3-hydroxy-5-[(5-nitrothien-2-yl)mercapto]-1,2,4-triazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl Isothiocyanate | HCID 5971 | — |
| Reactant | 2-Bromo-5-nitrothiazole | HCID 18211 | — |
| Reactant | HCID 178456608 | HCID 178456608 | — |
| Product | 4-Allyl-3-hydroxy-5-[(5-nitrothien-2-yl)mercapto]-1,2,4-triazole | HCID 178456609 | — |
Reaction Steps
The title compound was prepared in a similar manner described in Example 5 starting with allyl isothiocyanate. 4-Allyl-3-hydroxy-5-mercapto-1,2,4-triazole was reacted with 2-bromo-5-nitrothiazole as in Example 5. Crystallization from ethanol and water gave 4-allyl-3-hydroxy-5-[(5-nitrothien-2-yl)mercapto]-1,2,4-triazole as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05883110 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-83d20bb27f9c47cc9749fe636599c5e7 |
| Source note | uspto-grants-1999_03 |