HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → 2,3-Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]styrol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | 2,3,Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-styryl carboxylate | HCID 131719753 | — |
| Product | 2,3-Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]styrol | HCID 18359165 | 99.6% |
Reaction Steps
Using the procedure of Stage C of Example 40, 20 g of ester of Step B and 88 ml of diisobutylaluminium hydride were reacted to obtain 17.9 g of the expected product melting at 60° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05883248 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-d19ac2a94a624f8e8c45f02345055c36 |
| Source note | uspto-grants-1999_03 |