Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1418871Generated: October 31, 2026

HCID 10422857, compound → HCID 15411306, compound

https://huagongshe.com/reaction/1418871

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 10422857HCID 10422857—
Reactant7-Amino-2H-1,4-benzothiazin-3(4H)-oneHCID 12627419—
SolventEthanolHCID 702—
ProductHCID 15411306HCID 1541130692.5%

Reaction Steps

A liquid mixture of 1.316 g (5 mmol) of 3-(2-quinolinylmethoxy)benzaldehyde, 0.901 g (5 mmol) of 7-amino-3,4-dihydro-2H-1,4-benzothiazin-3-one and 70 ml of EtOH was heated under reflux and stirring for 24 hours. The mixture was then allowed to cool down. The precipitate was collected by filtration, whereby 1.969 g of the title compound were obtained as pale yellow powder (yield: 92.3%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05885987
Source datasetuspto-grants-1999_03
ORD IDord-3c551406941f44b8b6c42b2a9349dd32
Source noteuspto-grants-1999_03