1-(3,4-Dichlorophenyl)piperazine → HCID 9929605, compound

HRID 1418886Notes

Reaction equation

HRID 1418886 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N:9]2[CH2:14][CH2:13][NH:12][CH2:11][CH2:10]2)[CH:5]=[CH:6][C:7]=1[Cl:8].C[C:16]1[CH:17]=[C:18]([N:23]2CC[NH:26][CH2:25][CH2:24]2)[CH:19]=[CH:20][C:21]=1[CH3:22]>>[Cl:1][C:2]1[CH:3]=[C:4]([N:9]2[CH2:14][CH2:13][N:12]([CH2:22][C:21]3[CH:20]=[C:19]4[C:18](=[CH:17][CH:16]=3)[NH:23][CH2:24][CH2:25][NH:26]4)[CH2:11][CH2:10]2)[CH:5]=[CH:6][C:7]=1[Cl:8]

Participants

3

Reactant 2

HCID 936011-(3,4-Dichlorophenyl)piperazineHCID 27237821-(3,4-Xylyl)piperazine

Product 1

HCID 9929605HCID 9929605, compound

Procedure

Example 7 was prepared according to Example 2 except that in Step A 1-(3,4-dichlorophenyl)piperazine is substituted for 1-(3,4-dimethylphenyl)piperazine; mp 139°-141° C.

Workup

  1. customExample 7 was prepared

Sources & evidence

ORD record
ord-02fb331b06f1453eb8358bf11a432fe0
Source dataset
uspto-grants-1999_03
Patent number
US05885994

Reaction notes

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