1-(m-Tolyl)piperazine → HCID 9883643, compound

HRID 1418888Notes

Reaction equation

HRID 1418888 reaction equation
[C:1]1([CH3:13])[CH:6]=[CH:5][CH:4]=[C:3]([N:7]2[CH2:12][CH2:11][NH:10][CH2:9][CH2:8]2)[CH:2]=1.C[C:15]1[CH:16]=[C:17]([N:22]2CC[NH:25][CH2:24][CH2:23]2)[CH:18]=[CH:19][C:20]=1[CH3:21]>>[C:1]1([CH3:13])[CH:6]=[CH:5][CH:4]=[C:3]([N:7]2[CH2:8][CH2:9][N:10]([CH2:21][C:20]3[CH:19]=[C:18]4[C:17](=[CH:16][CH:15]=3)[NH:22][CH2:23][CH2:24][NH:25]4)[CH2:11][CH2:12]2)[CH:2]=1

Participants

3

Reactant 2

HCID 831111-(m-Tolyl)piperazineHCID 27237821-(3,4-Xylyl)piperazine

Product 1

HCID 9883643HCID 9883643, compound

Procedure

Example 9 was prepared according to Example 2 except that in Step A 1-(m-tolyl)piperazine is substituted for 1-(3,4-dimethylphenyl)piperazine; mp 135°-136° C.

Workup

  1. customExample 9 was prepared

Sources & evidence

ORD record
ord-29ac15f8c60544f193c3e74f2d2669e0
Source dataset
uspto-grants-1999_03
Patent number
US05885994

Reaction notes

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