HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-ethoxy-2-isocyanato- → N-(2-hydroxy-4-nitrophenyl)-N'-(2-ethoxyphenyl)urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-ethoxy-2-isocyanato- | HCID 79374 | — |
| Reactant | 2-Amino-5-Nitrophenol | HCID 4984721 | — |
| Product | N-(2-hydroxy-4-nitrophenyl)-N'-(2-ethoxyphenyl)urea | HCID 21184629 | 81.7% |
Reaction Steps
N-(2-Hydroxy-4-nitrophenyl)-N'-(2-ethoxyphenyl)urea was prepared from 2-hydroxy 4-nitro aniline (500 mg, 3.24 mmol) and 2-ethoxy phenyl isocyanate (3.24 mmol) according to the procedure in General Method B. The product was purified by dilution with methylene chloride and precipitation with hexanes. Filtering afforded the title compound(0.84 g, 81%). EI-MS m/z 318(M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05886044 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-0ed7436c6f5a4b82adfe98c5811793fc |
| Source note | uspto-grants-1999_03 |