3,3'-Iminodipropionitrile → HCID 86753985, compound

HRID 1419504Notes

Reaction equation

HRID 1419504 reaction equation
[NH:1]([CH2:6][CH2:7][C:8]#[N:9])[CH2:2][CH2:3][C:4]#[N:5].[CH:10]1([CH:13]=O)[CH2:12][CH2:11]1>>[C:4]([CH2:3][CH2:2][N:1]([CH2:6][CH2:7][C:8]#[N:9])[CH2:13][CH:10]1[CH2:12][CH2:11]1)#[N:5]

Participants

3

Reactant 2

HCID 81493,3'-IminodipropionitrileHCID 123114Cyclopropanecarboxaldehyde

Product 1

HCID 86753985HCID 86753985, compound

Procedure

The title compound was prepared from 3,3'-iminodipropionitrile and cyclopropanecarboxaldehyde by the method described in Example 1 in comparable yield. 1H NMR (CDCl3, 200 MHz) 2.86 (t, J=7.0 Hz, 4H), 2.42 (t, J=7.0 Hz, 4H), 2.39 (d, J=7.2 Hz, 1H), 0.75 (m, 1H), 0.45 (m, 2H), 0.06 (m, 2H).

Sources & evidence

ORD record
ord-709109760c65436294835a168c823658
Source dataset
uspto-grants-1999_03
Patent number
US05886185

Reaction notes

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