5-Nitrothiophene-2-carboxaldehyde → HCID 15410666, compound

HRID 1419535Notes

Reaction equation

HRID 1419535 reaction equation
[N+:1]([C:4]1[S:5][C:6]([CH:9]=O)=[CH:7][CH:8]=1)([O-:3])=[O:2].[C:11]1([CH2:17][CH2:18][CH2:19][NH:20][S:21]([CH2:24][C:25]#[N:26])(=[O:23])=[O:22])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[N+:1]([C:4]1[S:5][C:6](/[CH:9]=[C:24](/[S:21]([NH:20][CH2:19][CH2:18][CH2:17][C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=2)(=[O:23])=[O:22])\[C:25]#[N:26])=[CH:7][CH:8]=1)([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 782815-Nitrothiophene-2-carboxaldehydeHCID 15410494(3-Phenyl-n-propyl)aminosulfonylacetonitrile

Product 1

HCID 15410666HCID 15410666, compound

Procedure

Reaction of 2-nitrothiophen-5-carboxaldehyde and (3-phenyl-n-propyl)aminosulfonylacetonitrile as in Example 1 gave (E)-3-(2-nitrothien-5-yl)-2-[(3-phenyl-n-propyl)aminosulfonyl]acrylonitrile

Sources & evidence

ORD record
ord-0cb07fb6bb09489fb96bb6982967060b
Source dataset
uspto-grants-1999_03
Patent number
US05886195

Reaction notes

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