HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-(Decyloxy)phenyl)boronic acid → 2-(4-Decyloxyphenyl)-9,10-difluoro-7-butyl-phenanthrene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-(Decyloxy)phenyl)boronic acid | HCID 10612601 | — |
| Reactant | 9,1 0-Difluoro-2-bromo-7-butylphenanthrene | HCID 17887502 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 2-(4-Decyloxyphenyl)-9,10-difluoro-7-butyl-phenanthrene | HCID 53749106 | — |
Reaction Steps
From 9,1 0-difluoro-2-bromo-7-butylphenanthrene and 4-decyloxyphenyl-boronic acid by means of palladium-catalyzed Suzuki coupling (in analogy to Acc. Chem. Res. 1982, 15, 178). The crude product is purified by column chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05888422 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-85da385c4d0e4688982864e9774447ea |
| Source note | uspto-grants-1999_03 |