HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diphosgene → HCID 53769317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diphosgene | HCID 10426 | — |
| Reactant | HCID 53853228 | HCID 53853228 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 53769317 | HCID 53769317 | — |
Reaction Steps
5 g (17 mmol) of 7-amino-4,6-dichloro-2-(methylsulfonyl)benzothiazole and 17 g (85 mmol) of diphosgene in 200 ml of toluene were refluxed for 8 hours, after which the reaction mixture was evaporated down.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05888940 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-497b350acbaf453d94905e118a79958e |
| Source note | uspto-grants-1999_03 |