2',4'-Dihydroxyacetophenone → HCID 54403197, compound

HRID 1419731Notes

Reaction equation

HRID 1419731 reaction equation
[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7](Cl)=[O:8])=[CH:5][C:4]=1[CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[CH3:17][C:18]([C:20]1[CH:21]=[CH:22][C:23]([OH:27])=[CH:24][C:25]=1[OH:26])=[O:19].CC(C1C(O)=CC(O)=CC=1O)=O>>[OH:26][C:25]1[CH:24]=[C:23]([OH:27])[CH:22]=[C:21]2[C:20]=1[C:18](=[O:19])[CH:17]=[C:7]([C:6]1[CH:10]=[CH:11][C:3]([O:2][CH3:1])=[C:4]([CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])[CH:5]=1)[O:8]2

Participants

4

Reactant 3

HCID 69902',4'-DihydroxyacetophenoneHCID 680732',4',6'-TrihydroxyacetophenoneHCID 53903089HCID 53903089, compound

Product 1

HCID 54403197HCID 54403197, compound

Procedure

Using the procedure described in Preparation B, replacing 3-cyclopentyloxy-4-methoxybenzoyl chloride by 4-methoxy-3-pentylbenzoyl chloride, and 2,4-dihydroxyacetophenone by 2,4,6-trihydroxyacetophenone, the expected compound is obtained.

Workup

  1. customdescribed in Preparation B

Sources & evidence

ORD record
ord-02c091705bb0411ea422dc2174f6316b
Source dataset
uspto-grants-1999_03
Patent number
US05889003

Reaction notes

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