Allyl Isothiocyanate → HCID 178456994, compound

HRID 1419745Notes

Reaction equation

HRID 1419745 reaction equation
Cl.[NH2:2][C:3]1[CH:7]=[C:6]([Cl:8])[S:5][C:4]=1[S:9]([NH2:12])(=[O:11])=[O:10].[CH2:13]([N:16]=[C:17]=S)[CH:14]=[CH2:15]>>[CH2:13]([NH:16][C:17]1[NH:2][C:3]2[CH:7]=[C:6]([Cl:8])[S:5][C:4]=2[S:9](=[O:10])(=[O:11])[N:12]=1)[CH:14]=[CH2:15]

Participants

3

Reactant 2

HCID 5971Allyl IsothiocyanateHCID 688206263-Amino-5-chlorothiophene-2-sulfonamide hydrochloride

Product 1

HCID 178456994HCID 178456994, compound

Procedure

The title compound was prepared from 3-amino-5-chlorothiophene-2-sulfonamide hydrochloride and allyl isothiocyanate by a procedure analogous to the procedure described in example 3Bc-d; mp 217°-221° C.; 1H-NMR (DMSO-d6): δ 3.83 (distorted t, 2H), 5.08-5.27 (m, 2H), 5.75-5.99 (m, 1H), 7.07 (s, 1H), 7.49 (br. t, 1H), 11.1 (s, 1H).

Sources & evidence

ORD record
ord-e7c2e79730ec4228978ca5fd169bcd01
Source dataset
uspto-grants-1999_03
Patent number
US05889002

Reaction notes

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