Tetradecyl isothiocyanate → HCID 178443155, compound

HRID 1419748Notes

Reaction equation

HRID 1419748 reaction equation
Cl.[NH2:2][C:3]1[CH:7]=[C:6]([Cl:8])[S:5][C:4]=1[S:9]([NH2:12])(=[O:11])=[O:10].[CH2:13]([N:27]=[C:28]=S)[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]>>[Cl:8][C:6]1[S:5][C:4]2[S:9](=[O:10])(=[O:11])[N:12]=[C:28]([NH:27][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])[NH:2][C:3]=2[CH:7]=1

Participants

3

Reactant 2

HCID 137861Tetradecyl isothiocyanateHCID 688206263-Amino-5-chlorothiophene-2-sulfonamide hydrochloride

Product 1

HCID 178443155HCID 178443155, compound

Procedure

The title compound was prepared from 3-amino-5-chlorothiophene-2-sulfonamide hydrochloride and n-tetradecyl isothiocyanate by a procedure analogous to the procedure described in example 3Bc-d; mp 157°-158° C.; 1H-NMR (DMSO-d6): δ 0.85 (distorted t, 3H), 1.25 (m, 22H), 1.50 (m, 2H), 3.19 (q, 2H), 7.05 (s, 1H), 7.26 (br. s, 1H), 10.95 (br. s, 1H).

Sources & evidence

ORD record
ord-19770b44dbc74615983594f2415fc634
Source dataset
uspto-grants-1999_03
Patent number
US05889002

Reaction notes

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