Methyl isothiocyanate → HCID 178482508, compound

HRID 1419749Notes

Reaction equation

HRID 1419749 reaction equation
Cl.[NH2:2][C:3]1[CH:7]=[C:6]([Cl:8])[S:5][C:4]=1[S:9]([NH2:12])(=[O:11])=[O:10].[CH3:13][N:14]=[C:15]=S>>[Cl:8][C:6]1[S:5][C:4]2[S:9](=[O:10])(=[O:11])[N:12]=[C:13]([NH:14][CH3:15])[NH:2][C:3]=2[CH:7]=1

Participants

3

Reactant 2

HCID 11167Methyl isothiocyanateHCID 688206263-Amino-5-chlorothiophene-2-sulfonamide hydrochloride

Product 1

HCID 178482508HCID 178482508, compound

Procedure

The title compound was prepared from 3-amino-5-chlorothiophene-2-sulfonamide hydrochloride and methyl isothiocyanate by a procedure analogous to the procedure described in example 3Bc-d; mp >190° C. decomp.; 1H-NMR (DMSO-d6): δ 2.75 (s, 3H), 7.02 (s, 1H), 7.25 (br, 1H), 11.3 (br s, 1H).

Sources & evidence

ORD record
ord-d096de819bb44cd1ad33abd3c300d87f
Source dataset
uspto-grants-1999_03
Patent number
US05889002

Reaction notes

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