Octyl isothiocyanate → HCID 178443611, compound

HRID 1419751Notes

Reaction equation

HRID 1419751 reaction equation
Cl.[NH2:2][C:3]1[CH:7]=[C:6]([Cl:8])[S:5][C:4]=1[S:9]([NH2:12])(=[O:11])=[O:10].[CH2:13]([N:21]=[C:22]=S)[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]>>[Cl:8][C:6]1[S:5][C:4]2[S:9](=[O:10])(=[O:11])[N:12]=[C:22]([NH:21][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])[NH:2][C:3]=2[CH:7]=1

Participants

3

Reactant 2

HCID 78161Octyl isothiocyanateHCID 688206263-Amino-5-chlorothiophene-2-sulfonamide hydrochloride

Product 1

HCID 178443611HCID 178443611, compound

Procedure

The title compound was prepared from 3-amino-5-chlorothiophene-2-sulfonamide hydrochloride and n-octyl isothiocyanate by a procedure analogous to the procedure described in example 3Bc-d; mp >190° C. decomp.; 1H-NMR (DMSO-d6): δ 0.85 (t, 3H), 1.28 (m, 10H), 1.50 (m, 2H), 3.18 (q, 2H), 7.03 (s, 1H), 7.25 (br. s, 1H), 10.2 (br. s, 1H).

Sources & evidence

ORD record
ord-ea378babe50949a58a823849f54c687e
Source dataset
uspto-grants-1999_03
Patent number
US05889002

Reaction notes

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