(R)-sec-butylamine → HCID 178456035, compound

HRID 1419758Notes

Reaction equation

HRID 1419758 reaction equation
Cl[C:2]1[NH:7][C:6]2[CH:8]=[C:9]([Cl:11])[S:10][C:5]=2[S:4](=[O:13])(=[O:12])[N:3]=1.[C@H:14]([NH2:18])([CH2:16][CH3:17])[CH3:15]>O>[C@H:14]([NH:18][C:2]1[NH:7][C:6]2[CH:8]=[C:9]([Cl:11])[S:10][C:5]=2[S:4](=[O:13])(=[O:12])[N:3]=1)([CH2:16][CH3:17])[CH3:15]

Participants

4

Reactant 2

HCID 2724537(R)-sec-butylamineHCID 118320583,6-Dichloro-4h-thieno[3,2-e][1,2,4]thiadiazine 1,1-dioxide

Product 1

HCID 178456035HCID 178456035, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The title compound was prepared from 3,6-dichloro-4H-thieno[3,2-e]-1,2,4-thiadiazine 1,1-dioxide and (R)-(-)-sec-butylamine by a procedure analogous to the procedure described in example 1Bb; mp 215°-220° C. (water), 1H-NMR (DMSO-d6): δ 0.88 (t. 3H), 1.11 (d, 3H), 1.48 (m, 2H), 3.69 (m, 1H), 7.07 (s, 1H), 7.14 (br. s, 1H), 10.75 (br. s, 1H).

Sources & evidence

ORD record
ord-e6fa143ef5d540938ccd82e6b0d9f04b
Source dataset
uspto-grants-1999_03
Patent number
US05889002

Reaction notes

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