4-Methyloxybenzyl chloride → HCID 54420297, compound

HRID 1419771Notes

Reaction equation

HRID 1419771 reaction equation
Cl[C:2]1[CH:11]=[C:10]2[C:5]([C:6]([OH:15])=[C:7]([C:12]([OH:14])=[O:13])[CH:8]=[N:9]2)=[CH:4][CH:3]=1.[CH3:16][O:17][C:18]1[CH:25]=[CH:24][C:21]([CH2:22]Cl)=[CH:20][CH:19]=1.Cl.Cl.[NH:28]1[CH2:33][CH2:32][CH:31]([CH:34]2[CH2:39][CH2:38][NH:37][CH2:36][CH2:35]2)[CH2:30][CH2:29]1>>[CH3:16][O:17][C:18]1[CH:25]=[CH:24][C:21]([CH2:22][N:9]2[C:10]3[C:5](=[CH:4][CH:3]=[C:2]([N:28]4[CH2:33][CH2:32][CH:31]([CH:34]5[CH2:39][CH2:38][NH:37][CH2:36][CH2:35]5)[CH2:30][CH2:29]4)[CH:11]=3)[C:6](=[O:15])[C:7]([C:12]([OH:14])=[O:13])=[CH:8]2)=[CH:20][CH:19]=1

Participants

4

Procedure

Using 7-chloro-4-hydroxyquinoline-3-carboxylic acid, 4-methoxybenzyl chloride and 4,4'-bipiperidine dihydrochloride, the same procedure as in Reference Example 5 and Production Example 1 was followed to yield the title compound as a colorless crystal.

Sources & evidence

ORD record
ord-442e1e71b0e541089c5be615d87e3612
Source dataset
uspto-grants-1999_03
Patent number
US05889009

Reaction notes

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