Benzyl isocyanate → HCID 53908269, compound

HRID 1419847Notes

Reaction equation

HRID 1419847 reaction equation
[NH:1]1[CH2:6][CH2:5][CH:4]([O:7][C:8]2[CH:15]=[CH:14][C:11]([CH:12]=[O:13])=[CH:10][CH:9]=2)[CH2:3][CH2:2]1.[CH2:16]([N:23]=[C:24]=[O:25])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[CH2:16]([NH:23][C:24]([N:1]1[CH2:2][CH2:3][CH:4]([O:7][C:8]2[CH:15]=[CH:14][C:11]([CH:12]=[O:13])=[CH:10][CH:9]=2)[CH2:5][CH2:6]1)=[O:25])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

Participants

3

Reactant 2

HCID 76639Benzyl isocyanateHCID 450368384-[(Piperidin-4-yl)oxy]benzaldehyde

Product 1

HCID 53908269HCID 53908269, compoundYield 80%

Procedure

The title compound (0.2 g, 80%) was prepared as a white solid from 4-(piperidin-4-yloxy)benzaldehyde (0.25 g) and benzyl isocyanate (0.084 ml), in a similar manner to that described in preparation 14.

Workup

  1. customdescribed in preparation 14

Sources & evidence

ORD record
ord-f1a6dc25e002448faf5147575c6076fa
Source dataset
uspto-grants-1999_03
Patent number
US05889025

Reaction notes

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