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HRID1420097

反应详情

EQUATION

反应方程式

HRID 1420097 的结构方程式

REACTANTS

反应物

2
结构：CC(C)[C@H](N)C(=O)O
HCID6287

L-Valine

C5H11NO2

结构：O=C(Cl)c1ccccc1SSc1ccccc1C(=O)Cl
HCID88164

2,2'-Dithiodibenzoyl chloride

C14H8Cl2O2S2

PRODUCTS

生成物

1
结构：CC(C)C(NC(=O)c1ccccc1SSc1ccccc1C(=O)NC(C(=O)O)C(C)C)C(=O)O
HCID465364

未命名化合物

PROCEDURE

实验过程

Using the method employed in Preparation 30, 17.8 g (0.15 mol) of D,L valine was reacted with 17.2 g (0.05 mol) of 2,2'-dithiobisbenzoyl chloride to produce 11.4 g of the title compound after recrystallization from acetic acid, mp 226.5°-227.5° C.