HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide → HCID 178418472, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide | HCID 53745902 | — |
| Reactant | Sodium hydrogen sulphide | HCID 86586439 | — |
| Product | HCID 178418472 | HCID 178418472 | 63.6% |
Reaction Steps
Using the procedure in Preparation 34, 6.4 g (0.02 mol) of 4-chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide was reacted with 4.8 g (0.066 mol) of sodium hydrogen sulfide to afford 4.2 g of the title compound, mp 178°-180° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05889034 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-bd7d005154984883b5bd36cf3a93424c |
| Source note | uspto-grants-1999_03 |