Sodium Chloride → HCID 86754017, compound
Reaction equation
Cl.[S:2]([Cl:8])([CH2:5][CH2:6][NH2:7])(=[O:4])=[O:3].[N-:9]=[N+:10]=[N-:11].[Na+].[Cl-].[Na+]>O>[ClH:8].[S:2]([N:9]=[N+:10]=[N-:11])([CH2:5][CH2:6][NH2:7])(=[O:4])=[O:3]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 5 °C
Procedure
Tauryl chloride hydrochloride and sodium azide were reacted with one another in a ratio of 1:1 in water. For this purpose, the calculated stoichiometric amount of sodium azide was dissolved in water and the solution was cooled to 5° C. Tauryl chloride hydrochloride was added while stirring and the reaction mixture was stirred for 15 min. By stripping off the water, a solid mixture of crystalline sodium chloride and taurylazide hydrochloride was obtained.
Workup
- stirringthe reaction mixture was stirred for 15 min
Sources & evidence
- ORD record
- ord-565a5de21273402ca3b2b091199d3602
- Source dataset
- uspto-grants-1999_03
- Patent number
- US05889183
Reaction notes
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