Furan → HCID 131721836, compound

HRID 1420469Notes

Reaction equation

HRID 1420469 reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[CH:2]1.[CH2:6]([OH:71])[C@H:7]1[O:12][C@@H:11]2[O:13][C@H:14]3[C@H:19]([OH:20])[C@@H:18]([OH:21])[C@@H:17]([O:22][C@H:23]4[C@H:28]([OH:29])[C@@H:27]([OH:30])[C@@H:26]([O:31][C@H:32]5[C@H:37]([OH:38])[C@@H:36]([OH:39])[C@@H:35]([O:40][C@H:41]6[C@H:46]([OH:47])[C@@H:45]([OH:48])[C@@H:44]([O:49][C@H:50]7[C@H:56]([OH:57])[C@@H:55]([OH:58])[C@@H:53]([O:54][C@H:8]1[C@H:9]([OH:70])[C@H:10]2[OH:69])[O:52][C@@H:51]7[CH2:59][OH:60])[O:43][C@@H:42]6[CH2:61][OH:62])[O:34][C@@H:33]5[CH2:63][OH:64])[O:25][C@@H:24]4[CH2:65][OH:66])[O:16][C@@H:15]3[CH2:67][OH:68]>>[O:1]1[CH:5]=[CH:4][CH:3]=[CH:2]1.[CH2:61]([OH:62])[C@H:42]1[O:43][C@@H:44]2[O:49][C@H:50]3[C@H:56]([OH:57])[C@@H:55]([OH:58])[C@@H:53]([O:54][C@H:8]4[C@H:9]([OH:70])[C@@H:10]([OH:69])[C@@H:11]([O:13][C@H:14]5[C@H:19]([OH:20])[C@@H:18]([OH:21])[C@@H:17]([O:22][C@H:23]6[C@H:28]([OH:29])[C@@H:27]([OH:30])[C@@H:26]([O:31][C@H:32]7[C@H:37]([OH:38])[C@@H:36]([OH:39])[C@@H:35]([O:40][C@H:41]1[C@H:46]([OH:47])[C@H:45]2[OH:48])[O:34][C@@H:33]7[CH2:63][OH:64])[O:25][C@@H:24]6[CH2:65][OH:66])[O:16][C@@H:15]5[CH2:67][OH:68])[O:12][C@@H:7]4[CH2:6][OH:71])[O:52][C@@H:51]3[CH2:59][OH:60]

Participants

3

Reactant 2

HCID 8029FuranHCID 444913Alpha-Cyclodextrin

Product 1

HCID 131721836HCID 131721836, compound

Procedure

20 ml of saturated α-cyclodextrin solution were mixed with 1 ml of furan and ultrasounded for 3 minutes in the ultrasonic bath. The resulting difficultly soluble complex was obtained through filtration and dried via calcium chloride.

Workup

  1. customThe resulting difficultly soluble complex was obtained through filtration
  2. dry with materialdried via calcium chloride

Sources & evidence

ORD record
ord-56a17c5395c8425fb3dd8a77f38b770d
Source dataset
uspto-grants-2000_06
Patent number
US06071496

Reaction notes

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