1-Phenyl-1,3,8-triazaspiro(4.5)decan-4-one → HCID 18782452, compound

HRID 1420666Notes

Reaction equation

HRID 1420666 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[S:10][CH2:9][CH2:8][C:7](=[N:11]O)[C:6]=2[CH:13]=1.[C:14]1([N:20]2[C:24]3([CH2:29][CH2:28]N[CH2:26][CH2:25]3)[C:23](=[O:30])[NH:22][CH2:21]2)[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[Cl:1][C:2]1[CH:13]=[C:6]2[C:5](=[CH:4][CH:3]=1)[S:10][CH2:9][CH2:8][CH:7]2[N:11]1[CH2:28][CH2:29][C:24]2([N:20]([C:14]3[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=3)[CH2:21][NH:22][C:23]2=[O:30])[CH2:25][CH2:26]1

Participants

3

Reactant 2

HCID 705561-Phenyl-1,3,8-triazaspiro(4.5)decan-4-oneHCID 53396375HCID 53396375, compound

Product 1

HCID 18782452HCID 18782452, compound

Procedure

The title compound, m.p. 164-166° C. dec. and MS: m/e=414.2 (M+H+) was prepared in accordance with the general method of example 11 from 6-chloro-2,3-dihydro-4H-1-benzothiopyran-4-one oxime and 1-phenyl-1,3,8-triazaspiro[4.5]decan-4-one.

Sources & evidence

ORD record
ord-fa298e7378ff4b63acffc653d953acd8
Source dataset
uspto-grants-2000_06
Patent number
US06071925

Reaction notes

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