1-Phenyl-1,3,8-triazaspiro(4.5)decan-4-one → HCID 18782450, compound

HRID 1420667Notes

Reaction equation

HRID 1420667 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[C:8](=[N:12]O)[CH2:7][CH2:6][CH2:5]2.[C:14]1([N:20]2[C:24]3([CH2:29][CH2:28]N[CH2:26][CH2:25]3)[C:23](=[O:30])[NH:22][CH2:21]2)[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[ClH:1].[Cl:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[CH:8]([N:12]1[CH2:28][CH2:29][C:24]3([N:20]([C:14]4[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=4)[CH2:21][NH:22][C:23]3=[O:30])[CH2:25][CH2:26]1)[CH2:7][CH2:6][CH2:5]2

Participants

3

Reactant 2

HCID 705561-Phenyl-1,3,8-triazaspiro(4.5)decan-4-oneHCID 73471953HCID 73471953, compound

Product 1

HCID 18782450HCID 18782450, compound

Procedure

The title compound, m.p.>250° C. and MS: m/e=396.2 (M+H+) was prepared in accordance with the general method of example 11 from 6-chloro-3,4-dihydro-1(2H)-naphthalenone oxime and 1-phenyl-1,3,8-triazaspiro[4.5]decan-4-one.

Sources & evidence

ORD record
ord-2f41285bc0864a6391124f2e9cd2ae00
Source dataset
uspto-grants-2000_06
Patent number
US06071925

Reaction notes

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