1-Phenyl-1,3,8-triazaspiro(4.5)decan-4-one → HCID 18782367, compound

HRID 1420668Notes

Reaction equation

HRID 1420668 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]23O[C:6]2([CH:12]=1)[C:7](=O)[CH2:8][CH2:9][O:10]3.[C:14]1([N:20]2[C:24]3([CH2:29][CH2:28][NH:27][CH2:26][CH2:25]3)[C:23](=[O:30])[NH:22][CH2:21]2)[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[ClH:1].[Cl:1][C:2]1[CH:12]=[C:6]2[C:5](=[CH:4][CH:3]=1)[O:10][CH2:9][CH2:8][CH:7]2[N:27]1[CH2:26][CH2:25][C:24]2([N:20]([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[CH2:21][NH:22][C:23]2=[O:30])[CH2:29][CH2:28]1

Participants

3

Reactant 2

HCID 705561-Phenyl-1,3,8-triazaspiro(4.5)decan-4-oneHCID 86755442HCID 86755442, compound

Product 1

HCID 18782367HCID 18782367, compound

Procedure

The title compound, m.p.>250° C. and MS: m/e=398.2 (M+H+) was prepared in accordance with the general method of example 11 from 6-chloro-2,3 -dihydro-4H-1-benzopyran-4-one oxide and 1-phenyl-1,3,8-triazaspiro[4.5]decan-4-one.

Sources & evidence

ORD record
ord-7d2c7c411f4b4f8a982f240e53162a84
Source dataset
uspto-grants-2000_06
Patent number
US06071925

Reaction notes

Loading…