HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonate → HCID 131721849, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonate | HCID 85570 | — |
| Reactant | 1-(Dibutylamino)ethanol | HCID 22057057 | — |
| Reactant | HCID 131721850 | HCID 131721850 | — |
| Product | HCID 131721849 | HCID 131721849 | 53% |
Reaction Steps
The reaction was carried out in a manner analogous to that for (dimethylaminoethyl)di(2-propyl)cyclopentadiene, the tosylate of N,N-di-n-butylaminoethanol being prepared in situ. The conversion was 94%. The non-geminal di-n-butylaminoethyldi(2-propyl)-cyclopentadiene was obtained by distillation with a yield of 53%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06072067 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-adea1d02aea14a9795eba6886ced40a1 |
| Source note | uspto-grants-2000_06 |