HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 5327699, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | HCID 18780283 | HCID 18780283 | — |
| Solvent | Ammonia | HCID 222 | — |
| Product | HCID 5327699 | HCID 5327699 | — |
Reaction Steps
A solution of 804 mg of 3-(1-methyl-3-indolyl)-4-[1-methyl-2-(methylthio)-3-indolyl]furan-2,5-dione in 12 ml of DMF and 50 ml of 33% aqueous ammonia was heated to 130° C. for 2 hours. The product was filtered off and dried to give 675 mg of 3-(1-methyl-3-indolyl)-4-[1-methyl-2-(methylthio)-3-indolyl]-1H-pyrrole-2,5-dione, m.p. 281°-283° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE036736 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-609a3330878748daa014093dc5acf0f4 |
| Source note | uspto-grants-2000_06 |