HCID 54033015, compound → HCID 29938575, compound

HRID 1421253Notes

Reaction equation

HRID 1421253 reaction equation
[C:1]1([CH:11]([CH2:16][C:17]([OH:19])=[O:18])[CH2:12][C:13]([OH:15])=[O:14])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1.[CH2:20](O)CC(C)C.CC(C)=O.O>>[CH3:20][O:14][C:13](=[O:15])[CH2:12][C@H:11]([C:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1)[CH2:16][C:17]([OH:19])=[O:18]

Participants

3

Reactant 2

HCID 54033015HCID 54033015, compoundHCID 87805135HCID 87805135, compound

Product 1

HCID 29938575HCID 29938575, compound

Procedure

Formula C16H16O4. Yield 62%; TLC (isoamyl alcohol-acetone-H2O 5:2:2) Rf. 0.65 (N.B.: 3-(1-naphthyl) glutaric acid has Rf. 0.52 in the same eluent).

Sources & evidence

ORD record
ord-8fe3271627a648529fd2ba9d566f6737
Source dataset
uspto-grants-2000_06
Patent number
US06075033

Reaction notes

Loading…