Pentane → HCID 131720371, compound

Participants

Reaction Steps

((Tetramethylcyclopentadienyl)dimethylsilyl)-(4-fluorophenyl)amine in diethyl ether solvent and butyl lithium 2.5 M in hexane solvent were combined in equivalent amounts. A white precipitate formed. Pentane was added to the slurry. The precipitate was filtered, washed with pentane and dried. 1H NMR (THF-d8) δ 7.28 (m, 2.0), 6.77 (m, 2), 3.27 (s, 2.7), 2.05 (s, 5.2), 2.01(s, 5.2), 0.44 (s, 4.6)

Provenance & Evidence