HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → Sodium 4-methoxybenzene-1-sulfinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | 4-Methoxybenzenesulfonyl chloride | HCID 7401 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Sodium 4-methoxybenzene-1-sulfinate | HCID 23680956 | 97% |
Reaction Steps
Sodiumiodide (21.76 grams, 145.2 mmol) and 4-methoxybenzenesulfonyl chloride (10.0 grams, 48.39 mmol) were combined in dry acetone (dried over MgSO4 and filtered) (200 ml) and stirred at room temperature overnight. Collected fine white solids via suction filtration. Dried on high vacuum giving 9.11 grams of sodium 4-methoxybenzenesulfinate as a pale yellow fine powder (97% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06077864 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-d7eca36944064be6b9d865c9807cf873 |
| Source note | uspto-grants-2000_06 |