Acetonitrile → HCID 18347910, compound

HRID 1421682Notes

Reaction equation

HRID 1421682 reaction equation
Br[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([CH2:9][Br:10])[CH:4]=1.[C:11]1(=[O:21])[NH:15][C:14](=[O:16])[C:13]2=[CH:17][CH:18]=[CH:19][CH:20]=[C:12]12.[K].[C:23](#N)C>>[C:11]1(=[O:21])[N:15]([CH2:2][C:3]2[CH:8]=[CH:7][CH:6]=[C:5]([CH2:9][Br:10])[C:4]=2[CH3:23])[C:14](=[O:16])[C:13]2=[CH:17][CH:18]=[CH:19][CH:20]=[C:12]12

Participants

4

Reactant 3

HCID 6342AcetonitrileHCID 69373Benzene, 1,3-bis(bromomethyl)-HCID 24194345Phthalimide potassium salt

Product 1

HCID 18347910HCID 18347910, compound

Procedure

α,α'-Dibromo-m-xylene is refluxed with potassium phthalimide (1.0 equivalent) in acetonitrile to give the title compound.

Sources & evidence

ORD record
ord-5282524fcebc468a82c448d0ca68d33f
Source dataset
uspto-grants-2000_06
Patent number
US06077954

Reaction notes

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