HCID 86755476, compound → HCID 86755477, compound

Participants

Reaction Steps

A mixture of cis-1-benzyl-2,3,3a,4,9,9a-hexahydro-1H-benz[f]indole (1.20 g, 4.6 mmol) and palladium hydroxide (0.91 g, 8.6 mmol) in degassed methanol (90 ml) was hydrogenated at 50° C. and 50 psi pressure for 5 h. The resultant mixture was cooled and filtered through kieselguhr. The filtrate was evaporated in vacuo to give the title compound as a colourless oil (0.55 g, 70%).

Provenance & Evidence