HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(6-Decyloxy-2-naphthoyloxy)benzoic acid benzyl ester → HCID 19069990, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(6-Decyloxy-2-naphthoyloxy)benzoic acid benzyl ester | HCID 19093197 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19069990 | HCID 19069990 | 97.5% |
Reaction Steps
To 37.6 g (0.07 mol) of the 4-(6-decyloxy-2-naphthoyloxy)benzoic acid benzyl ester obtained in the first stage was added 3.76 g of 5% palladium/carbon, and further added 188 g of THF. Then, hydrogen gas was blown into the mixture. The resultant mixture was stirred overnight and filtered to obtain 30.6 g of 4-(6-decyloxy-2-naphthoyloxy)benzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05725798 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-4f7cf5895f954e1fa345200adbbaaa61 |
| Source note | uspto-grants-1998_03 |