HCID 848930, compound → HCID 29074119, compound

HRID 1422020Notes

Reaction equation

HRID 1422020 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]([NH:11][NH:12][C:13]([C:15]2[S:16][CH:17]=[CH:18][CH:19]=2)=O)=[S:10])=[CH:4][CH:3]=1.COC1C=CC(NC(NNC(C2SC=CC=2)=O)=S)=CC=1>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:13]([C:15]3[S:16][CH:17]=[CH:18][CH:19]=3)=[N:12][NH:11][C:9]2=[S:10])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 848930HCID 848930, compoundHCID 18708934HCID 18708934, compound

Product 1

HCID 29074119HCID 29074119, compoundYield 57.9%

Procedure

By substituting 2 g of N1-(4-bromophenylaminothiocarbonyl)-N2-(thien-2-carbonyl)hydrazine for the N1-(4-methoxyphenylaminothiocarbonyl)-N2-(thien-2-carbonyl)hydrazine in the method of Example 97, 1.1 g of the title compound is obtained as an off-white solid.

Sources & evidence

ORD record
ord-7d93b070fa0f4df88b6b5f1a4aaf6284
Source dataset
uspto-grants-2000_06
Patent number
US06080772

Reaction notes

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