HCID 86584760, compound → HCID 21969221, compound

HRID 1422131Notes

Reaction equation

HRID 1422131 reaction equation
C(O)(=O)/C=C/C(O)=O.[Cl:9][C:10]1[CH:29]=[CH:28][C:13]2[C:14]([C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=3[CH:23]([CH2:25][C:26]#[CH:27])[NH2:24])=[N:15][O:16][C:12]=2[CH:11]=1>CO>[ClH:9].[O:16]1[C:12]2[CH:11]=[CH:10][CH:29]=[CH:28][C:13]=2[C:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=2[C@@H:23]([CH2:25][CH:26]=[CH2:27])[NH2:24])=[N:15]1

Participants

3

Reactant 1

HCID 86584760HCID 86584760, compound

Product 1

HCID 21969221HCID 21969221, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

(+)-2-(6-chloro-1,2-benzisoxazol-3-yl)-a-2-propynyl-benzenemethanamine (E)-butenedioate (2:1 salt), melting at 176-179° C., a (c=0.5 in methanol) +20.7,

Sources & evidence

ORD record
ord-244ffdf6f3f44685a9e97214a23a1365
Source dataset
uspto-grants-2000_06
Patent number
US06080773

Reaction notes

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