HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 18778875, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 18778867 | HCID 18778867 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18778875 | HCID 18778875 | — |
Reaction Steps
A solution of 5-(3-Cyclopentyloxy-4-methoxyphenyl)pyrimidine (1.37 g) and 3-chloroperoxybenzoic acid (50.60%) (1.75 g) in dichloromethane (35 ml) was stirred at RT and the reaction followed by t.l.c. After 5 days, the reaction mixture was partitioned three times between dichloromethane (50 ml) and 10% aqueous Na2SO3 solution (50 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06080790 |
| Source dataset | uspto-grants-2000_06 |
| ORD ID | ord-64b97472af0c45a485f4f8e0b0a05e2d |
| Source note | uspto-grants-2000_06 |