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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1422165Generated: November 2, 2026

m-Chloroperbenzoic acid → HCID 18778875, compound

https://huagongshe.com/reaction/1422165

Reaction equation

Participants

RoleNameHCIDCharge
Reactantm-Chloroperbenzoic acidHCID 70297—
ReactantHCID 18778867HCID 18778867—
SolventDichloromethaneHCID 6344—
ProductHCID 18778875HCID 18778875—

Reaction Steps

A solution of 5-(3-Cyclopentyloxy-4-methoxyphenyl)pyrimidine (1.37 g) and 3-chloroperoxybenzoic acid (50.60%) (1.75 g) in dichloromethane (35 ml) was stirred at RT and the reaction followed by t.l.c. After 5 days, the reaction mixture was partitioned three times between dichloromethane (50 ml) and 10% aqueous Na2SO3 solution (50 ml).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06080790
Source datasetuspto-grants-2000_06
ORD IDord-64b97472af0c45a485f4f8e0b0a05e2d
Source noteuspto-grants-2000_06