Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Nitrate | HCID 24434 | — |
| Reactant | HCID 23298010 | HCID 23298010 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 18706433 | HCID 18706433 | — |
Reaction Steps
20 ml of sulfuric acid are cooled to 0° C. and then 5 g (13.8 mmol) of 7-bromo-5-bromomethyl-2,3-dimethoxy-quinoxaline are added. After a further 15 minutes, 1.46 g (1.05 equiv.) of potassium nitrate are added and the mixture is stirred for 15 hours at 20° C. The mixture is poured onto ice, and the solid is filtered off and washed with water. The title compound is obtained in the form of a beige solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06080743 |
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| Source dataset | uspto-grants-2000_06 |
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| ORD ID | ord-cfe9b306f43c472ea1c7d5ecce923c92 |
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| Source note | uspto-grants-2000_06 |
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