HCID 18706711, compound → HCID 18706590, compound

HRID 1422243Notes

Reaction equation

[N+:1]([C:4]1[CH:13]=[C:12]2[C:7]([NH:8][C:9](=[O:15])[C:10](=[O:14])[NH:11]2)=[C:6]([CH2:16][NH:17][C:18]([NH:20][C:21]2[CH:26]=CC(OC(F)(F)F)=CC=2)=[O:19])[CH:5]=1)([O-:3])=[O:2].[C:32]([O:35][CH2:36][CH3:37])(=[O:34])C.CO>>[N+:1]([C:4]1[CH:13]=[C:12]2[C:7]([NH:8][C:9](=[O:15])[C:10](=[O:14])[NH:11]2)=[C:6]([CH2:16][NH:17][C:18]([NH:20][CH2:21][CH2:26][C:32]([O:35][CH2:36][CH3:37])=[O:34])=[O:19])[CH:5]=1)([O-:3])=[O:2]

Participants

Reactant 2

HCID 18706711HCID 18706711, compound

HCID 21584119Ethylacetate methanol

Product 1

HCID 18706590HCID 18706590, compound

Procedure

1-(7-nitro-2,3-dioxo-1,2,3,4-tetrahydroquinoxalin-5-ylmethyl)-3-(4-trifluoromethyloxyphenyl)-urea, FAB-MS: M+ =439; TLC: ethyl acetate/methanol (3:1) Rf =0.50.

Sources & evidence

ORD record: ord-de3530558a8f450fb360d2e37a285a4b
Source dataset: uspto-grants-2000_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06080743

Reaction notes

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