Ethylacetate methanol → HCID 54398257, compound

HRID 1422245Notes

Reaction equation

[N+:1]([C:4]1[CH:13]=[C:12]2[C:7]([NH:8][C:9](=[O:15])[C:10](=[O:14])[NH:11]2)=[C:6]([CH2:16][NH:17][C:18](=[O:26])[C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][C:20]=2O)[CH:5]=1)([O-:3])=[O:2].[C:27]([O:30]CC)(=[O:29])[CH3:28].CO>>[N+:1]([C:4]1[CH:13]=[C:12]2[C:7]([NH:8][C:9](=[O:15])[C:10](=[O:14])[NH:11]2)=[C:6]([CH2:16][NH:17][C:18](=[O:26])[C:19]2[CH:24]=[CH:23][CH:22]=[C:21]([O:30][C:27](=[O:29])[CH3:28])[CH:20]=2)[CH:5]=1)([O-:3])=[O:2]

Participants

Reactant 2

HCID 21584119Ethylacetate methanol

HCID 44364031HCID 44364031, compound

Product 1

HCID 54398257HCID 54398257, compound

Procedure

N-(7-nitro-2,3-dioxo-1,2,3,4-tetrahydroquinoxalin-5-ylmethyl)-(2-hydroxy)-benzoic acid amide, ESCl+ -MS: (M+H)+ =357; TLC: ethyl acetate/methanol (1:1+2% acetic acid) Rf 0.33.

Sources & evidence

ORD record: ord-55f676928c9145709515ce5c577c055c
Source dataset: uspto-grants-2000_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06080743

Reaction notes

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