HCID 70272022, compound → HCID 56985744, compound

HRID 1422247Notes

Reaction equation

HRID 1422247 reaction equation
[N+:1]([C:4]1[CH:13]=[C:12]2[C:7]([NH:8][C:9](=[O:15])[C:10](=[O:14])[NH:11]2)=[C:6]([CH2:16][N:17](C)[C:18](=[O:24])[CH2:19][CH2:20][C:21]([OH:23])=[O:22])[CH:5]=1)([O-:3])=[O:2]>C(Cl)Cl.CO.C(O)(=O)C>[N+:1]([C:4]1[CH:13]=[C:12]2[C:7]([NH:8][C:9](=[O:15])[C:10](=[O:14])[NH:11]2)=[C:6]([CH2:16][NH:17][C:18](=[O:24])[C:19]2[C:20](=[CH:13][CH:4]=[CH:5][CH:6]=2)[C:21]([OH:23])=[O:22])[CH:5]=1)([O-:3])=[O:2]

Participants

3

Reactant 1

HCID 70272022HCID 70272022, compound

Product 1

HCID 56985744HCID 56985744, compound

Reagents, catalysts & solvents 1

HCID 21877243DCM MeOH AcOHSolvent

Procedure

N-(7-nitro-2,3-dioxo-1,2,3,4-tetrahydroquinoxalin-5-ylmethyl)-N-methyl-succinic acid amide, FAB-MS: M+ =350; TLC: methylene chloride/methanol/acetic acid (80:18:2) Rf =0.46.

Sources & evidence

ORD record
ord-ba6de78d6f9c47d6935c1d5b7f0cb233
Source dataset
uspto-grants-2000_06
Patent number
US06080743

Reaction notes

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