HCID 18706770, compound → HCID 18706452, compound

HRID 1422249Notes

Reaction equation

HRID 1422249 reaction equation
[BrH:1].[N+:2]([C:5]1[CH:14]=[C:13]2[C:8]([NH:9][C:10](=[O:16])[C:11](=[O:15])[NH:12]2)=[C:7]([CH2:17][NH:18][CH:19]2CCS(=O)(=O)C2)[CH:6]=1)([O-:4])=[O:3]>CO.C(O)(=O)C>[BrH:1].[N+:2]([C:5]1[CH:14]=[C:13]2[C:8]([NH:9][C:10](=[O:16])[C:11](=[O:15])[NH:12]2)=[C:7]([CH2:17][NH:18][CH3:19])[CH:6]=1)([O-:4])=[O:3]

Participants

3

Reactant 1

HCID 18706770HCID 18706770, compound

Product 1

HCID 18706452HCID 18706452, compound

Reagents, catalysts & solvents 1

HCID 10129899Acetic acid methanolSolvent

Procedure

N-(7-nitro-2,3-dioxo-1,2,3,4-tetrahydroquinoxalin-5-ylmethyl)-N-(1,1-dioxo-2,3,4,5-tetrahydro-thien-3-yl)-amine hydrobromide, FAB-MS: M+ =354; TLC: methanol/acetic acid (9:1) Rf =0.69;

Sources & evidence

ORD record
ord-1e8b663b265b40808798515f4160d828
Source dataset
uspto-grants-2000_06
Patent number
US06080743

Reaction notes

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