Acetic acid methanol → HCID 18706564, compound

HRID 1422250Notes

Reaction equation

HRID 1422250 reaction equation
[BrH:1].[N+:2]([C:5]1[CH:14]=[C:13]2[C:8]([NH:9][C:10](=[O:16])[C:11](=[O:15])[NH:12]2)=[C:7]([CH2:17][NH:18][CH:19](C2C=CC=CC=2)CC(O)=O)[CH:6]=1)([O-:4])=[O:3].CO.[C:32]([OH:35])(=O)[CH3:33]>>[BrH:1].[N+:2]([C:5]1[CH:14]=[C:13]2[C:8]([NH:9][C:10](=[O:16])[C:11](=[O:15])[NH:12]2)=[C:7]([CH2:17][N:18]([CH3:19])[CH2:33][CH2:32][OH:35])[CH:6]=1)([O-:4])=[O:3]

Participants

3

Reactant 2

HCID 10129899Acetic acid methanolHCID 70271843HCID 70271843, compound

Product 1

HCID 18706564HCID 18706564, compound

Procedure

3-[N-(7-nitro-2,3-dioxo-1,2,3,4-tetrahydroquinoxalin-5-ylmethyl)amino]-3-phenyl-propionic acid hydrobromide, ESCl+ -MS: (M+H)+ =385; TLC: methanol/acetic acid (9:1) Rf =0.34;

Sources & evidence

ORD record
ord-b99ed54312314db9bdb24bd9ff458405
Source dataset
uspto-grants-2000_06
Patent number
US06080743

Reaction notes

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