Water → HCID 18779192, compound

Participants

Reaction Steps

The phenol from step A (1.72 g, 9.35 mmol), CS2CO3 (3.6 g, 10.5 mmol) and allylbromide (0.9 mL, 10.3 mmol) in DMF (47 nmL) were stirred at room temperature for 48 h. The mixture was poured into water and extracted with EtOAc, washed with water (3×), brine, dried and evaporated to give the title compound as an oil.

Provenance & Evidence