Chlorobenzene → HCID 18779196, compound

Participants

Reaction Steps

To a stirred solution of BCl3 (1M in p-xylene; 6.7 mL, 6.7 mmol) in chlorobenzene at -15° C. was added the allyl ether from step B (1.48 g, 6.6 mmol) in 5 mL of chlorobenzene. After 1 h at -15° C., the mixture was poured into ice/MeOH, extracted with Et2O (3×), washed with saturated NaHCO3, water then brine. The dried solution was evaporated to give the title compound as an oil.

Provenance & Evidence