HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1-Benzothiophen-3-yl)boronic acid → HCID 59408908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1-Benzothiophen-3-yl)boronic acid | HCID 2776344 | — |
| Reactant | HCID 86643463 | HCID 86643463 | — |
| Product | HCID 59408908 | HCID 59408908 | — |
Reaction Steps
Following the procedure of Example 15d, (R)-4-(2-(2-chloro-9-(tetrahydrofuran-3-yl)-9H-purin-6-ylamino)ethyl)phenol (c) was reacted with benzo[b]thiophen-3-ylboronic acid (22.3 mg, 0.125 mmol). The crude residue was purified by reverse-phase preparative HPLC to afford the title compound as an off-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08927281B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-a9272923e6084e0ebb3fcfd41c10233b |
| Source note | uspto-grants-2015_01 |