Methyl chloroformate → HCID 52919656, compound

Participants

Reaction Steps

Prepared using the same procedure described in Example 89 from (S)-3-benzyl-1-(3-cyclobutoxy-4-methoxy-phenyl)-piperazine (188 mg, 0.535 mmol), diisopropylethylamine (200 μL, 1.15 mmol), and methyl chloroformate (62 μL, 0.81 mmol) to afford the title compound as a yellow solid (107 mg, 49%). LC/MS (Method B) 4.17 min, [M+1]+ 411.

Provenance & Evidence